2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

Base Information

Chemical Name:2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene
CAS No.:19822-34-5
Molecular Formula:C₇H₂ClF₃N₂O₆S
Molecular Weight:334.617
Hs Code.:

Synonyms:2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

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Chemical Property of 2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

Chemical Property:

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Technology Process of 2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

There total 4 articles about 2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78914-94-0
4-methoxyphenyl trifluoromethylsulfide

: 19822-34-5
2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 35percent aq. H₂O₂ / acetic acid / 48 h / 50 °C

2: 93 percent / 98percent H₂SO₄, HNO₃ / 8 h / 100 °C

3: 1.) pyridine hydrochloride, 2.) POCl₃ / 1.) from 115 deg C to 120 deg C, 2.) reflux, 30 min

With sulfuric acid; dihydrogen peroxide; nitric acid; pyridine hydrochloride; trichlorophosphate; In acetic acid;
DOI:10.1055/s-1997-1390

Reference yield:

: 19822-29-8
2,6-dinitro-4-((trifluoromethyl)sulfonyl)anisole

: 19822-34-5
2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

Guidance literature:: With pyridine hydrochloride; trichlorophosphate; Yield given. Multistep reaction; 1.) 115-120 deg C; 2.) reflux for 0.5 h.;

Reference yield:

: 15183-74-1
1-methoxy-4-((trifluoromethyl)sulfonyl)benzene

: 19822-34-5
2,6-dinitro-4-trifluoromethylsulfonylchlorobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 98percent H₂SO₄, HNO₃ / 8 h / 100 °C

2: 1.) pyridine hydrochloride, 2.) POCl₃ / 1.) from 115 deg C to 120 deg C, 2.) reflux, 30 min

With sulfuric acid; nitric acid; pyridine hydrochloride; trichlorophosphate;
DOI:10.1055/s-1997-1390