(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

Base Information

Chemical Name:(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline
CAS No.:1105064-57-0
Molecular Formula:C₂₃H₂₉NO₄
Molecular Weight:383.488
Hs Code.:

Synonyms:(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

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Chemical Property of (RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

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Technology Process of (RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

There total 1 articles about (RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1105064-42-3
2-(trifluoroacetyl)-1,2,3,4-tetrahydro-1-(4',5'-dimethoxy-2'-(2''-propenyl)phenyl)methyl-6,7-dimethoxyisoquinoline

: 1105064-57-0
(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

Guidance literature:: With water; potassium carbonate; In methanol; at 20 ℃; for 18h;
DOI:10.1016/j.tet.2008.10.052

Reference yield: 79.0%

: 108-30-5
succinic acid anhydride

: 1105064-57-0
(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

: 1105064-58-1
1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline 2-(4-oxo)butanoic acid

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2008.10.052

Reference yield: 62.0%

: 1105064-57-0
(RS) 1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline

: 1105064-58-1
1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4',5'-dimethoxy-2'-(2-propenyl)phenyl)methylisoquinoline 2-(4-oxo)butanoic acid

: 1185180-18-0
C₅₀H₆₀N₂O₁₀

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.094