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Technology Process of (CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

(CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

Base Information
  • Chemical Name:(CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4
  • CAS No.:208589-76-8
  • Molecular Formula:C11H19N2O2Pd*C32H12BF24
  • Molecular Weight:1180.92
  • Hs Code.:
(CH<sub>3</sub>CO)Pd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2<sup>(1+)</sup>*B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4<sup>(1-)</sup>=CH<sub>3</sub>COPd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4

Synonyms:(CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

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Chemical Property of (CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4
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Technology Process of (CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

There total 1 articles about (CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)
350016-97-6

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)

carbon monoxide
201230-82-2

carbon monoxide

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
79060-88-1

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

(CH<sub>3</sub>CO)Pd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2<sup>(1+)</sup>*B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4<sup>(1-)</sup>=CH<sub>3</sub>COPd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4
208589-76-8

(CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

Guidance literature:
In dichloromethane; byproducts: NaCl; (N2); mixing boron compd. and palladium complex in CH2Cl2 satd. with CO at -40°C under CO atmosphere, slow warming to 0°C, stirring for 1 h; filtration through Celite, evapn. by bubbling CO, treatment with hexane satd. with CO; elem. anal.;
DOI:10.1021/om000971n

Reference yield: 90.0%

(CH<sub>3</sub>CO)Pd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2<sup>(1+)</sup>*B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4<sup>(1-)</sup>=CH<sub>3</sub>COPd(CO)(CH<sub>3</sub>)2CHNCHCHNCH(CH<sub>3</sub>)2B[C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2]4
208589-76-8

(CH3CO)Pd(CO)(CH3)2CHNCHCHNCH(CH3)2(1+)*B[C6H3(CF3)2]4(1-)=CH3COPd(CO)(CH3)2CHNCHCHNCH(CH3)2B[C6H3(CF3)2]4

[Pd(CH<sub>3</sub>)(carbonyl)(1,4-diisopropyl-1,4-diaza-1,3-butadiene)]<sup>(1+)</sup>[B(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4]<sup>(1-)</sup>
208589-78-0

[Pd(CH3)(carbonyl)(1,4-diisopropyl-1,4-diaza-1,3-butadiene)](1+)[B(3,5-(CF3)2C6H3)4](1-)

Guidance literature:
With nitrogen; In dichloromethane; byproducts: CO; (N2); bubbling N2 at -15°C for 10 min through a soln. of palladium complex in CH2Cl2; filtration through Celite, evapn. at -15°C, dissolving in CH2Cl2,pptn., washing with hexane at -15°C; elem. anal.;
DOI:10.1021/om000971n
upstream raw materials:

(i-Pr-1,4-diazabutadiene)(metyl)chloropalladium(II)

carbon monoxide

sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

Downstream raw materials:

[Pd(CH3)(carbonyl)(1,4-diisopropyl-1,4-diaza-1,3-butadiene)](1+)[B(3,5-(CF3)2C6H3)4](1-)

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