acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester

Base Information

• Chemical Name: acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester
• CAS No.: 926290-89-3
• Molecular Formula: C₁₄H₁₆N₄O₂
• Molecular Weight: 272.307

Synonyms:acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester

Chemical Property of acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester

Chemical Property:

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Technology Process of acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester

There total 1 articles about acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Tetramethylenetetrazole (7465-48-7) + benzaldehyde (100-52-7) + acetyl chloride (75-36-5) → acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester (926290-89-3)

Guidance literature:

Tetramethylenetetrazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

benzaldehyde; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

acetyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1016/j.tetlet.2006.11.125

Reference yield:

acetic acid phenyl-(5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridin-8-yl)-methyl ester (926290-89-3) → 8-benzylidene-5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridine (954154-12-2)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2006.11.125

upstream raw materials:

Tetramethylenetetrazole

benzaldehyde

acetyl chloride

Downstream raw materials:

8-benzylidene-5,6,7,8-tetrahydro-tetrazolo[1,5-a]pyridine

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