C₂₄H₂₉NO₂

Base Information

Chemical Name:C₂₄H₂₉NO₂
CAS No.:1531590-65-4
Molecular Formula:C₂₄H₂₉NO₂
Molecular Weight:363.5
Hs Code.:

C<sub>24</sub>H<sub>29</sub>NO<sub>2</sub>

Synonyms:C₂₄H₂₉NO₂

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Chemical Property of C₂₄H₂₉NO₂

Chemical Property:

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Technology Process of C₂₄H₂₉NO₂

There total 2 articles about C₂₄H₂₉NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75-30-9
2-iodo-propane

: 1531590-64-3
C₂₁H₂₃NO₂

: 1531590-65-4
C₂₄H₂₉NO₂

Guidance literature:: C₂₁H₂₃NO₂; With lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; at -78 - 0 ℃; for 1.5h; Inert atmosphere;

2-iodo-propane; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201309449

Reference yield:

: 53293-00-8
hex-5-ynoic acid

: 550-58-3,20616-51-7,20616-52-8,46797-67-5,53176-60-6,54852-85-6,75196-48-4,90365-73-4
(1R,2S)-1,2-diphenyl-2-(N-methyl)aminoethanol

: 1531590-65-4
C₂₄H₂₉NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2.1: lithium chloride; lithium diisopropyl amide / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/anie.201309449

Reference yield:

: 1531590-65-4
C₂₄H₂₉NO₂

: 1531590-72-3
C₂₂H₂₉NO₆

: 1531590-73-4
C₂₂H₂₉NO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetra(n-butyl)ammonium hydroxide / tert-butyl alcohol; water / 36 h / 20 - 100 °C / Inert atmosphere

1.2: pH <= 1 / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 20.5 h / 20 °C / Inert atmosphere

4.1: S-alpine borane / tetrahydrofuran / 11 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

6.1: N,N,N,N,N,N-hexamethylphosphoric triamide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; indium iodide / tetrahydrofuran / 8 h / 0 °C / Inert atmosphere

7.1: 4-nitro-benzoic acid; [1,3-bis(2,6-diisopropylphenyl)-1H-imidazol-2-(3H)-ylidene]gold(I)chloride; silver hexafluoroantimonate / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; silver hexafluoroantimonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; indium iodide; [1,3-bis(2,6-diisopropylphenyl)-1H-imidazol-2-(3H)-ylidene]gold(I)chloride; S-alpine borane; tetra(n-butyl)ammonium hydroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 4-nitro-benzoic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/anie.201309449