dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

Base Information

Chemical Name:dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate
CAS No.:1428540-11-7
Molecular Formula:C₂₁H₂₄N₂O₆
Molecular Weight:400.431
Hs Code.:

Synonyms:dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

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Chemical Property of dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

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Technology Process of dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

There total 3 articles about dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944392-68-1
dimethyl 5-(pinacolboryl)isophthalate

: 285119-72-4
(6-chloropyridin-3-ylmethyl)carbamic acid tert-butyl ester

: 1428540-11-7
dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In water; N,N-dimethyl-formamide; at 80 ℃; Inert atmosphere;
DOI:10.1039/c3cc41190g

Reference yield:

: 51839-15-7
5-iodo-isophthalic acid dimethyl ester

: 1428540-11-7
dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; sodium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41190g

Reference yield:

: 97004-04-1
5-(aminomethyl)-2-chloropyridine

: 1428540-11-7
dimethyl 5-(5-((tert-butoxycarbonylamino)methyl)pyridin-2-yl)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; N,N-dimethyl-formamide / 80 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41190g