(bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane

Base Information

• Chemical Name: (bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane
• CAS No.: 215111-88-9
• Molecular Formula: C₂₇H₅₀GeO₂Si₄
• Molecular Weight: 591.625
• Mol file: 215111-88-9.mol

Synonyms:(bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane

Chemical Property of (bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane

There total 1 articles about (bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

hexamesitylcyclotrigermane (107824-84-0) + tris-(trimethylsilyl)silane (1873-77-4) → (bis(trimethylsiloxy)(trimethylsilyl)silyl)dimesitylgermane (215111-88-9) + (dimesitylmethylgermyl)dimesitylgermane (156486-46-3)

Guidance literature:

With methylmagnesium bromide; ammonium chloride; In diethyl ether; toluene; Irradiation (UV/VIS); (Ar); photolysis (-78°C, 16 h), quenching by CH3MgBr, hydrolysis (aq.NH4Cl); extraction from water by diethyl ether, separation by preparative chromatography (Chromatotron, 8:92 dichloromethane/hexanes);

DOI:10.1021/ja981787k

upstream raw materials:

hexamesitylcyclotrigermane

tris-(trimethylsilyl)silane