hexamesitylcyclotrigermane

Base Information

Chemical Name:hexamesitylcyclotrigermane
CAS No.:107824-84-0
Molecular Formula:C₅₄H₆₆Ge₃
Molecular Weight:932.888
Hs Code.:

Synonyms:hexamesitylcyclotrigermane

Suppliers and Price of hexamesitylcyclotrigermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexamesitylcyclotrigermane

Chemical Property:

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Technology Process of hexamesitylcyclotrigermane

There total 3 articles about hexamesitylcyclotrigermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 96481-42-4
dichlorodimesitylgermane

: 107824-84-0
hexamesitylcyclotrigermane

Guidance literature:: With magnesium; magnesium bromide; In tetrahydrofuran; to mixt. of Mg, MgBr2 and THF was added a soln. of germane in THF and stirred for 2 h at room temp., mixt. hydrolysed with HCl; mixt. extd. with ether, ext. evapd., hexane added;
DOI:10.1039/c39870001514

Reference yield:

: 115385-07-4
tetrakis(2,4,6-trimethylphenyl)digermene

: 107824-84-0
hexamesitylcyclotrigermane

Guidance literature:: With 2,6-dimethylphenyl isonitrile; In tetrahydrofuran; at 20 ℃; for 120h; Reagent/catalyst; Inert atmosphere;
DOI:10.1002/chem.201602222

Reference yield:

: 100418-04-0
1,2-dichlorotetramesityldigermane

: 5599-27-9
dichloro(dimesityl)silane

: 107824-84-0
hexamesitylcyclotrigermane

: 136131-68-5
hexamesitylsiladigermirane

Guidance literature:: With naphthalen-1-yl-lithium; In 1,2-dimethoxyethane; soln. of dichlorodimesitylsilane and 1,2-dichlorotetramesityldigermane in dry DME is added to a cold (dry ice/acetone) suspension of lithium naphthalenide, stirred at -78°C (1 h); warmed to room temp. over 24 h; acidified (1 N HCl); extd. (Et2O); crystd. (hexane); not sepd.; NMR;
DOI:10.1021/om00056a004