2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

Base Information

Chemical Name:2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine
CAS No.:118656-33-0
Molecular Formula:C₂₇H₁₉Br₂N
Molecular Weight:517.263
Hs Code.:

2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenz<c,h>acridine

Synonyms:2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

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Chemical Property of 2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

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Technology Process of 2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

There total 1 articles about 2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 32281-97-3
7-bromo-3,4-dihydro-2H-naphthalen-1-one

: 116047-27-9
7-benzylidene-2-bromo-α-tetralone

: 118656-33-0
2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: 7-bromo-3,4-dihydro-2H-naphthalen-1-one; 7-benzylidene-2-bromo-α-tetralone; With boron trifluoride diethyl etherate; at 100 ℃; for 4h;

With ammonia; In methanol; dichloromethane; at 20 ℃; for 48h; Further stages.;
DOI:10.1016/j.jfluchem.2005.12.007

Reference yield: 62.0%

: 1582-24-7
pentafluorophenylboronic acid

: 118656-33-0
2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

: 2,12-bis(pentafluorophenyl)-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridine

Guidance literature:: With tri-tert-butyl phosphine; cesium fluoride; silver(l) oxide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 12h;
DOI:10.1016/j.jfluchem.2005.12.007

Reference yield: 60.0%

: 118656-33-0
2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine

: 2,12-diiodo-7-phenyl-5,6,8,9-tetrahydro-dibenzo[c,h]acridine

Guidance literature:: 2,12-Dibromo-7-phenyl-5,6,8,9-tetrahydrodibenzacridine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

With iodine; In tetrahydrofuran; hexane; for 4h; Further stages.;
DOI:10.1016/j.jfluchem.2005.12.007