3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

Base Information

Chemical Name:3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride
CAS No.:1345403-93-1
Molecular Formula:C₁₈H₂₀N₄S*ClH
Molecular Weight:360.911
Hs Code.:

Synonyms:3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

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Chemical Property of 3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

Chemical Property:

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Technology Process of 3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

There total 6 articles about 3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345403-96-4
4-(3-Methylsulfanyl-1-phenyl-1H-indazol-6-yl)-piperazine-1-carboxylic acid tert-butyl ester

: 1345403-93-1
3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 1345403-94-2
2-Amino-4-bromo-benzoic acid N'-phenyl-hydrazide

: 1345403-93-1
3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; sodium nitrite / ethanol; water / 76 °C

2: tetraphosphorus decasulfide / xylene / 1 h / 130 °C

3: caesium carbonate / acetonitrile / 20 °C

4: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / Reflux

5: hydrogenchloride / dichloromethane / 0 - 20 °C

With hydrogenchloride; tetraphosphorus decasulfide; caesium carbonate; sodium nitrite; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In ethanol; dichloromethane; water; toluene; acetonitrile; xylene;

Reference yield:

: 1332526-99-4
6-Bromo-1-phenyl-1,2-dihydro-indazol-3-one

: 1345403-93-1
3-(methylsulfanyl)-1-phenyl-6-piperazin-1-yl-1H-indazole hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: tetraphosphorus decasulfide / xylene / 1 h / 130 °C

2: caesium carbonate / acetonitrile / 20 °C

3: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / Reflux

4: hydrogenchloride / dichloromethane / 0 - 20 °C

With hydrogenchloride; tetraphosphorus decasulfide; caesium carbonate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In dichloromethane; toluene; acetonitrile; xylene;