bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

Base Information

Chemical Name:bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate
CAS No.:133192-47-9
Molecular Formula:C₃₃H₃₂NO₈P
Molecular Weight:601.593
Hs Code.:

Synonyms:bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

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Chemical Property of bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

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Technology Process of bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

There total 5 articles about bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 133192-46-8
bis(phenylmethyl) cis-4-hydroxy-1,2-piperidinedicarboxylate

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 133192-47-9
bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1021/jo00012a061

Reference yield:

: 133192-43-5
(1α,5α)-2-(phenylmethyl)-6-oxa-2-azabicyclo<3.2.1>octan-7-one

: 133192-47-9
bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / H₂ / 20percent Pd/C / 2.2 h / 2606.4 Torr

2: 84 percent / Et₃N / CH₂Cl₂ / 1 h / 5 °C

3: aq. 1N NaOH / dioxane / 18 h / Ambient temperature

4: Adogen-464 / CH₂Cl₂ / 96 h / Ambient temperature

5: 73 percent / Et₃N, (dimethylamino)pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With dmap; sodium hydroxide; Adogen-464; hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jo00012a061

Reference yield:

: 100-39-0
benzyl bromide

: 133192-47-9
bis(phenylmethyl) cis-4-(diphenylphosphonooxy)-1,2-piperidinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Adogen-464 / CH₂Cl₂ / 96 h / Ambient temperature

2: 73 percent / Et₃N, (dimethylamino)pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With dmap; Adogen-464; triethylamine; In dichloromethane;
DOI:10.1021/jo00012a061