methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Base Information

Chemical Name:methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate
CAS No.:1260144-21-5
Molecular Formula:C₁₅H₂₂N₂O₅S
Molecular Weight:342.416
Hs Code.:

Synonyms:methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

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Technology Process of methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

There total 4 articles about methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1260144-13-5
methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

: 1260144-21-5
methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: With hydrogen; acetic acid; palladium 10% on activated carbon; In 1,4-dioxane; ethyl acetate; at 20 ℃; for 5h; Inert atmosphere;

Reference yield:

: 111712-04-0
4-phenylmethoxybenzenesulfonic acid sodium salt

: 1260144-21-5
methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

2: triethylamine / dichloromethane / 18 h / 20 °C

3: hydrogen; acetic acid / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane / 5 h / 20 °C / Inert atmosphere

With oxalyl dichloride; hydrogen; acetic acid; triethylamine; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 87001-32-9
p-benzyloxybenzenesulfonyl chloride

: 1260144-21-5
methyl (S)-3-(4-hydroxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 18 h / 20 °C

2: hydrogen; acetic acid / palladium 10% on activated carbon / ethyl acetate; 1,4-dioxane / 5 h / 20 °C / Inert atmosphere

With hydrogen; acetic acid; triethylamine; palladium 10% on activated carbon; In 1,4-dioxane; dichloromethane; ethyl acetate;