methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Base Information

Chemical Name:methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate
CAS No.:1260144-13-5
Molecular Formula:C₂₂H₂₈N₂O₅S
Molecular Weight:432.541
Hs Code.:

Synonyms:methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

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Chemical Property of methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

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Technology Process of methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

There total 4 articles about methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1260206-59-4
methyl(S)-3-amino-2-piperidin-1-ylpropanoate

: 87001-32-9
p-benzyloxybenzenesulfonyl chloride

: 1260144-13-5
methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h;

Reference yield:

: 100-39-0
benzyl bromide

: 1260144-13-5
methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / isopropyl alcohol; water / 20 h / 70 °C

2: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

3: triethylamine / dichloromethane / 18 h / 20 °C

With oxalyl dichloride; triethylamine; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 111712-04-0
4-phenylmethoxybenzenesulfonic acid sodium salt

: 1260144-13-5
methyl(S)-3-(4-benzyloxybenzenesulfonylamino)-2-piperidin-1-ylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 18 h / -20 - 20 °C

2: triethylamine / dichloromethane / 18 h / 20 °C

With oxalyl dichloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;