(1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol

Base Information

• Chemical Name: (1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol
• CAS No.: 124263-12-3
• Molecular Formula: C₁₅H₂₄O₃
• Molecular Weight: 252.354

Synonyms:(1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol

Chemical Property of (1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol

Chemical Property:

Purity/Quality:

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Technology Process of (1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol

There total 61 articles about (1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(+/-)-1-(3-furyl)-(2α-hydroxy-2,6,6-trimethylcyclohexyl)ethanone (90987-31-8,124263-08-7,124263-09-8) → (+/-)-(αRS,1'RS,2'RS)-α-<(2'-hydroxy-2',6',6'-trimethylcyclohexyl)methyl>furan-3-methanol (69924-97-6,69979-79-9,69979-80-2,69979-81-3,124263-10-1,124263-11-2,124263-12-3)

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; -78 deg C, 2.5 h, r.t., overnight;

DOI:10.1039/P19850002463

Reference yield: 90.0%

(1'R,2'R)-1-(3-furyl)-2-(2'-hydroxy-2',6',6'-trimethylcyclohexyl)-1-ethanone (124263-09-8) → (1R,1'R,2'R)-1-(3-furyl)-2-(2-'hydroxy-2',6',6'-trimethylcyclohexyl)ethanol (124263-12-3)

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; 1.) - 78 deg C, 3 h 2.) - 78 deg C to room temperature, 12 h;

Reference yield: 69.0%

(+/-)-(αRS,3'SR,4'RS)-α-(3-furyl)-5,5-dimethyl-1-oxaspiro<2.5>octane-4-ethanol (69924-96-5,69979-76-6,69979-77-7,69979-78-8) → (+/-)-(αRS,1'SR,2'RS)-α-<(2'-hydroxy-2',6',6'-trimethylcyclohexyl)methyl>furan-3-methanol (69924-97-6,69979-79-9,69979-80-2,69979-81-3,124263-10-1,124263-11-2,124263-12-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;

DOI:10.1039/P19850002463

upstream raw materials:

(1'S,2'S)-1-(3-furyl)-2-(2'-hydroxy-2',6',6'-trimethylcyclohexyl)-1-ethanone

(-)-trans-tetrahydroactinidiolide

(+)-(S)-3-(tert-butyldimethylsiloxy)-2,2-dimethylcyclohexanone

(S)-4-(tert-butyldimethylsilyloxy)-3,3-dimethyl-1-cyclohexenecarbaldehyde

Downstream raw materials:

(+/-)-1-(3-furyl)-(2α-hydroxy-2,6,6-trimethylcyclohexyl)ethanone

(+/-)-(αRS,1'SR,2'SR)-α-<(2'-hydroxy-2',6',6'-trimethylcyclohexyl)methyl>furan-3-methanol

(+/-)-(αRS,1'RS,2'RS)-α-<(2'-hydroxy-2',6',6'-trimethylcyclohexyl)methyl>furan-3-methanol

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