Technology Process of 5-(2-benzamidoethyl)carbostyril
There total 10 articles about 5-(2-benzamidoethyl)carbostyril which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
p-toluenesulfonyl chloride;
In
chloroform;
for 1h;
Heating;
DOI:10.1021/jm00150a010
- Guidance literature:
-
Multi-step reaction with 7 steps
1: toluene / 1 h / Heating
2: AcOH / 0.5 h / Heating
3: 10.7 g / NaBH4 / methanol / 0.5 h / 25 °C
4: H2 / Raney Ni / methanol / 1 h / 25 °C / 2585.7 Torr
5: Et3N / CHCl3
6: 45 percent / 30percent H2O2 / acetic acid / 1 h / Heating
7: 44 percent / p-toluenesulfonyl chloride / CHCl3 / 1 h / Heating
With
sodium tetrahydroborate; hydrogen; dihydrogen peroxide; acetic acid; triethylamine; p-toluenesulfonyl chloride;
nickel;
In
methanol; chloroform; acetic acid; toluene;
DOI:10.1021/jm00150a010
- Guidance literature:
-
Multi-step reaction with 8 steps
1: MnO2 / CHCl3 / 3 h
2: toluene / 1 h / Heating
3: AcOH / 0.5 h / Heating
4: 10.7 g / NaBH4 / methanol / 0.5 h / 25 °C
5: H2 / Raney Ni / methanol / 1 h / 25 °C / 2585.7 Torr
6: Et3N / CHCl3
7: 45 percent / 30percent H2O2 / acetic acid / 1 h / Heating
8: 44 percent / p-toluenesulfonyl chloride / CHCl3 / 1 h / Heating
With
manganese(IV) oxide; sodium tetrahydroborate; hydrogen; dihydrogen peroxide; acetic acid; triethylamine; p-toluenesulfonyl chloride;
nickel;
In
methanol; chloroform; acetic acid; toluene;
DOI:10.1021/jm00150a010
