4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

Base Information

Chemical Name:4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine
CAS No.:1126632-95-8
Molecular Formula:C₁₅H₁₄F₃NO₂
Molecular Weight:297.277
Hs Code.:

Synonyms:4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

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Chemical Property of 4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

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Technology Process of 4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

There total 4 articles about 4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1126633-18-8
4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzonitrile

: 1126632-95-8
4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

Guidance literature:: With ammonia; hydrogen; Raney nickel; In methanol; at 20 ℃; for 3h; under 2585.81 Torr;

Reference yield:

: 1-benzyloxy-4-methoxy-2-trifluoromethyl-benzene

: 1126632-95-8
4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 4 h / 20 °C / 2585.81 Torr

2: potassium carbonate / dimethyl sulfoxide / 3 h / 120 °C

3: hydrogen; ammonia / Raney nickel / methanol / 3 h / 20 °C / 2585.81 Torr

With ammonia; hydrogen; potassium carbonate; palladium 10% on activated carbon; In methanol; dimethyl sulfoxide; ethyl acetate;

Reference yield:

: 127271-65-2
1-fluoro-4-methoxy-2-(trifluromethyl)benzene

: 1126632-95-8
4-(4-methoxy-2-trifluoromethyl-phenoxy)-benzylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C

1.2: 2.5 h / 20 - 100 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 4 h / 20 °C / 2585.81 Torr

3.1: potassium carbonate / dimethyl sulfoxide / 3 h / 120 °C

4.1: hydrogen; ammonia / Raney nickel / methanol / 3 h / 20 °C / 2585.81 Torr

With ammonia; hydrogen; sodium hydride; potassium carbonate; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; dimethyl sulfoxide; ethyl acetate;