(S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester

Base Information

• Chemical Name: (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester
• CAS No.: 848211-10-9
• Molecular Formula: C₂₆H₃₁Cl₂NO₉S
• Molecular Weight: 604.505

Synonyms:(S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester

Chemical Property of (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester

Chemical Property:

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Technology Process of (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester

There total 1 articles about (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-hydroxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester (848211-03-0) + methanesulfonyl chloride (124-63-0) → (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester (848211-10-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4.5h;

Reference yield:

pyrrolidine (123-75-1) + (S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-methanesulfonyloxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester (848211-10-9) → C29H36Cl2N2O6

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 12h; Heating / reflux;

upstream raw materials:

(S)-3-[4-(2,6-dichlorobenzyloxy)phenyl]-2-[((4R,5S)-5-hydroxymethyl-[1,3]dioxolane-4-carbonyl)amino]propionic acid tert-butyl ester

methanesulfonyl chloride

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