1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

Base Information

Chemical Name:1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol
CAS No.:109081-20-1
Molecular Formula:C₁₉H₂₇N₃O₇S
Molecular Weight:441.505
Hs Code.:

Synonyms:1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

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Technology Process of 1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

There total 1 articles about 1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 71696-37-2
2,3:5,6-di-O-isopropylidene-1,4-di-O-toluene-p-sulphonyl-D-glucitol

: 109081-20-1
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

Guidance literature:: With sodium azide; In water; N,N-dimethyl-formamide; for 4h; Heating;
DOI:10.1016/S0008-6215(00)90194-0

Reference yield:

: 109081-20-1
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

: 109081-28-9
1-amino-1-deoxy-2,3-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen sulfide / 1.) pyridine, water, 40 deg C, 2 h, 2.) pyridine, water

2: 74.6 percent / acetic acid / H₂O / 3 h / 100 °C

With hydrogen sulfide; acetic acid; In water;
DOI:10.1016/S0008-6215(00)90194-0

Reference yield:

: 64-19-7,77671-22-8
acetic acid

: 109081-20-1
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

: 109081-24-5
1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

Guidance literature:: With hydrogen sulfide; Yield given. Multistep reaction; 1.) pyridine, water, 40 deg C, 2 h, 2.) pyridine, water;
DOI:10.1016/S0008-6215(00)90194-0