1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

Base Information

Chemical Name:1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate
CAS No.:109081-24-5
Molecular Formula:C₂H₄O₂*C₁₉H₂₉NO₇S
Molecular Weight:475.56
Hs Code.:

Synonyms:1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

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Technology Process of 1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

There total 2 articles about 1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71696-37-2
2,3:5,6-di-O-isopropylidene-1,4-di-O-toluene-p-sulphonyl-D-glucitol

: 109081-24-5
1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium azide / dimethylformamide; H₂O / 4 h / Heating

2: 1.) hydrogen sulfide / 1.) pyridine, water, 40 deg C, 2 h, 2.) pyridine, water

With sodium azide; hydrogen sulfide; In water; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90194-0

Reference yield:

: 64-19-7,77671-22-8
acetic acid

: 109081-20-1
1-azido-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol

: 109081-24-5
1-amino-1-deoxy-2,3:5,6-di-O-isopropylidene-4-O-p-tolylsulfonyl-D-glucitol acetate

Guidance literature:: With hydrogen sulfide; Yield given. Multistep reaction; 1.) pyridine, water, 40 deg C, 2 h, 2.) pyridine, water;
DOI:10.1016/S0008-6215(00)90194-0