(S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

Base Information

• Chemical Name: (S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride
• CAS No.: 126662-27-9
• Molecular Formula: C₁₂H₂₄ClO₂PS₂
• Molecular Weight: 330.88

Synonyms:(S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

Chemical Property of (S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

Chemical Property:

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Technology Process of (S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

There total 2 articles about (S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-24-6) → (S)P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride (126662-27-9)

Guidance literature:

With chloro-trimethyl-silane; In ethanol; at -40 ℃;

DOI:10.1016/S0040-4020(98)00529-8

Reference yield:

(-)-menthol (2216-51-5) → (S)P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride (126662-27-9)

Guidance literature:

Multi-step reaction with 4 steps

1: Et₃N

2: H₂S, Et₃N

3: Et₃N

4: Me₃SiCl, EtOH

With chloro-trimethyl-silane; ethanol; hydrogen sulfide; triethylamine;

DOI:10.1039/c39890001694

Reference yield: 100.0%

morpholine (110-91-8,99108-56-2) + (S)P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride (126662-27-9) → (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-24-6)

Guidance literature:

In hexane; at 0 - 5 ℃;

DOI:10.1016/S0040-4020(98)00529-8

upstream raw materials:

(S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

(-)-menthol

Downstream raw materials:

(S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

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