(S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Base Information

• Chemical Name: (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester
• CAS No.: 126662-24-6
• Molecular Formula: C₁₆H₃₂NO₃PS₂
• Molecular Weight: 381.541

Synonyms:(S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Chemical Property of (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Chemical Property:

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Technology Process of (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

There total 5 articles about (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

morpholine (110-91-8,99108-56-2) + (S)P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride (126662-27-9) → (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-24-6)

Guidance literature:

In hexane; at 0 - 5 ℃;

DOI:10.1016/S0040-4020(98)00529-8

Reference yield:

Phosphorochloridous acid ethyl ester (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester → (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-24-6)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂S / hexane / 5 h / 0 - 5 °C

2: 1.5 g / Et₃N / hexane

With hydrogen sulfide; triethylamine; In hexane;

DOI:10.1016/S0040-4020(98)00529-8

Reference yield:

N-(chlorosulfanyl)morpholine (2958-89-6) + RP,SP hydrogen O-ethyl O-l-(-)-menthylphosphinothioate (139416-17-4) → (S)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-24-6) + (R)-Dithiophosphoric acid O-ethyl ester O'-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester (126662-25-7)

Guidance literature:

With triethylamine;

upstream raw materials:

morpholine

(S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

N-(chlorosulfanyl)morpholine

R_P,S_P hydrogen O-ethyl O-l-(-)-menthylphosphinothioate

Downstream raw materials:

(S)_P-Ethoxy-L-menthoxythioxaphosphoranesulphenyl chloride

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