C₂₉H₂₆Cl₂N₂O₄

Base Information

Chemical Name:C₂₉H₂₆Cl₂N₂O₄
CAS No.:554418-71-2
Molecular Formula:C₂₉H₂₆Cl₂N₂O₄
Molecular Weight:537.442
Hs Code.:

C<sub>29</sub>H<sub>26</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₉H₂₆Cl₂N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₆Cl₂N₂O₄

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Technology Process of C₂₉H₂₆Cl₂N₂O₄

There total 4 articles about C₂₉H₂₆Cl₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 201230-82-2
carbon monoxide

: C₂₀H₁₇Cl₂NO₃

: 103-69-5
N-ethyl-N-phenylamine

: 554418-71-2
C₂₉H₂₆Cl₂N₂O₄

: C₂₉H₂₆Cl₂N₂O₄

Guidance literature:: With di(rhodium)tetracarbonyl dichloride; oxygen; copper(II) dipivaloate; Trimethylacetic acid; In chlorobenzene; at 130 ℃; for 36h; under 760.051 Torr; Overall yield = 40 %;
DOI:10.1039/c7sc02181j

Reference yield:

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: 554418-71-2
C₂₉H₂₆Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: pyridine / dichloromethane / 1 h / 20 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 90 °C

4: copper(II) dipivaloate; Trimethylacetic acid; oxygen; di(rhodium)tetracarbonyl dichloride / chlorobenzene / 36 h / 130 °C / 760.05 Torr

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; di(rhodium)tetracarbonyl dichloride; oxygen; copper(II) dipivaloate; triethylamine; N-ethyl-N,N-diisopropylamine; Trimethylacetic acid; In dichloromethane; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1039/c7sc02181j

Reference yield:

: 938195-80-3
methyl N-(2,6-dichlorobenzoyl)-L-tyrosinate

: 554418-71-2
C₂₉H₂₆Cl₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 1 h / 20 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 90 °C

3: copper(II) dipivaloate; Trimethylacetic acid; oxygen; di(rhodium)tetracarbonyl dichloride / chlorobenzene / 36 h / 130 °C / 760.05 Torr

With pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; di(rhodium)tetracarbonyl dichloride; oxygen; copper(II) dipivaloate; N-ethyl-N,N-diisopropylamine; Trimethylacetic acid; In dichloromethane; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1039/c7sc02181j