N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate

Base Information

• Chemical Name: N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate
• CAS No.: 82444-68-6
• Molecular Formula: C₁₉H₃₄NO₂Si*ClO₄
• Molecular Weight: 436.021

Synonyms:N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate

Chemical Property of N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate

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Technology Process of N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate

There total 3 articles about N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

pivaloyl chloride (3282-30-2) + 3--2-propenyl>-amino>cyclohex-2-enone (87883-67-8) → N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate (82444-68-6)

Guidance literature:

With silver perchlorate; In acetonitrile; at 0 ℃; for 1h;

DOI:10.1021/jo00176a002

Reference yield:

3-(methylamino)-2-cyclohexen-1-one (55998-74-8) → N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate (82444-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 1h, reflux -> 25 deg C, 24h

2: 99 percent / AgClO₄ / acetonitrile / 1 h / 0 °C

With silver perchlorate; sodium hydride; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo00176a002

Reference yield:

3-trimethylsilyl-2-(methylsulphonyloxymethyl)prop-1-ene (74532-54-0) → N-<3-<(tert-butylcarbonyl)oxy>cyclohex-2-enylidene>-N-<2-<(trimethylsilyl)methyl>-2-propenyl>methylammonium perchlorate (82444-68-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / NaH / tetrahydrofuran / 1h, reflux -> 25 deg C, 24h

2: 99 percent / AgClO₄ / acetonitrile / 1 h / 0 °C

With silver perchlorate; sodium hydride; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo00176a002

upstream raw materials:

pivaloyl chloride

3--2-propenyl>-amino>cyclohex-2-enone

3-(methylamino)-2-cyclohexen-1-one

3-trimethylsilyl-2-(methylsulphonyloxymethyl)prop-1-ene

Downstream raw materials:

N-(3-methoxycyclohex-2-enylidene)-N-<2-<(trimethylsilyl)methyl>-2-propenyl>ammonium perchlorate

3-cyclohex-2-enone

3-cyclohex-2-enone

3--2-propenyl>-amino>cyclohex-2-enone

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