1,3-di-tert-butyl-5-methyl-2-phenoxybenzene

Base Information

• Chemical Name: 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene
• CAS No.: 1619243-69-4
• Molecular Formula: C₂₁H₂₈O
• Molecular Weight: 296.453
• Mol file: 1619243-69-4.mol

Synonyms:1,3-di-tert-butyl-5-methyl-2-phenoxybenzene

Chemical Property of 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene

There total 2 articles about 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

iodobenzene (591-50-4) + 2,6-di-tert-butyl-4-methyl-phenol (128-37-0) → 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene (1619243-69-4)

Guidance literature:

With copper(l) iodide; 1-(dimethylamino-1-yl-pyridin-2-yl-methyl)naphthalen-2-ol; potassium carbonate; In dimethyl sulfoxide; at 120 ℃; for 24h; Green chemistry;

DOI:10.1080/00397911.2014.903421

Reference yield:

2,6-di-tert-butyl-4-methyl-phenol (128-37-0) + dibenzoyl peroxide (94-36-0) → 1,3-di-tert-butyl-5-methyl-2-phenoxybenzene (1619243-69-4)

Guidance literature:

With copper acetylacetonate; α,α,α-trifluorotoluene; S,S-diphenylsulphoximine; at 130 ℃; for 15h; Inert atmosphere; Sealed tube;

DOI:10.1016/j.tetlet.2016.04.042

upstream raw materials:

iodobenzene

2,6-di-tert-butyl-4-methyl-phenol

dibenzoyl peroxide