5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine

Base Information

• Chemical Name: 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine
• CAS No.: 222992-24-7
• Molecular Formula: C₃₃H₃₁N₅O₆S
• Molecular Weight: 625.705

Synonyms:5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine

Chemical Property of 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine

Chemical Property:

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Technology Process of 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine

There total 1 articles about 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(fluorenylmethoxy)carbonyl chloride (28920-43-6) + 1-[(2R,3S,5R)-3-Amino-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-3-benzoyl-thiourea → 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine (222992-24-7)

Guidance literature:

With TEA; In 1,4-dioxane; for 0.5h;

DOI:10.1021/ja984212w

Reference yield:

N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine (222992-24-7) → 2-{N'-[3-amino-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-N''-benzoyl-guanidino}-acetamide

Guidance literature:

Multistep reaction;

DOI:10.1021/ja984212w

Reference yield:

N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + 5'-benzoylthiourea-3-(9-fluorenylmethoxycarbamoyl)-3',5'-deoxythymidine (222992-24-7) → 2-{N'-[3-{N'-[3-amino-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-N''-benzoyl-guanidino}-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-ylmethyl]-N''-benzoyl-guanidino}-acetamide

Guidance literature:

Multistep reaction;

DOI:10.1021/ja984212w

upstream raw materials:

(fluorenylmethoxy)carbonyl chloride

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