1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene

Base Information

• Chemical Name: 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene
• CAS No.: 1242540-03-9
• Molecular Formula: C₁₈H₂₀N₂O₂
• Molecular Weight: 296.369
• Mol file: 1242540-03-9.mol

Synonyms:1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene

Chemical Property of 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene

There total 1 articles about 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

3,3'-(1,4-phenylenebis(methylene))bis(4-hydroxypent-3-en-2-one) → 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene (1242540-03-9)

Guidance literature:

3,3'-(1,4-phenylenebis(methylene))bis(4-hydroxypent-3-en-2-one); With hydroxylamine hydrochloride; sodium hydroxide; In ethanol; for 3h; Reflux;

In water; pH=7;

DOI:10.1039/c0cc00826e

Reference yield: 93.0%

1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene (1242540-03-9) + silver perchlorate → [Ag2(1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene)3](ClO4)2

Guidance literature:

In methanol; to hot soln. ligand in MeOH soln. AgClO4 in MeOH was added; soln. was stood at room temp. overnight, ppt. was filtered, washed with MeOH; elem. anal.;

DOI:10.1039/c1dt10029g

Reference yield: 48.0%

silver tetrafluoroborate (14104-20-2) + 1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene (1242540-03-9) → [Ag2(1,4-bis((3,5-dimethylisoxazol-4-yl)methyl)benzene)3](BF4)2

Guidance literature:

In methanol; to hot soln. ligand in MeOH soln. AgBF4 in MeOH was added; soln. was stood at room temp. overnight, ppt. was filtered, washed with MeOH; elem. anal.;

DOI:10.1039/c1dt10029g