BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE

Base Information

• Chemical Name: BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE
• CAS No.: 116696-66-3
• Molecular Formula: C23H27 N O6
• Molecular Weight: 413.46
• Mol file: 116696-66-3.mol

Synonyms:BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE

Chemical Property of BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE

Chemical Property:

• Melting Point: 170-176°C
• Refractive Index: 1.584
• PSA: 75.25000
• LogP: 2.95290

Purity/Quality:

98%Min ^*data from raw suppliers

Benzyl2-Acetamido-4,6-O-benzylidene-2-deoxy-3-O-methyl-α-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE

There total 3 articles about BENZYL 2-ACETAMIDO-4,6-O-BENZYLIDENE-2-DEOXY-3-O-METHYL-ALPHA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside (13343-63-0) + methyl iodide (74-88-4) → benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methyl-α-D-glucopyranoside (116696-66-3)

Guidance literature:

With silver(l) oxide; In N,N-dimethyl-formamide; for 6h; Ambient temperature;

DOI:10.1016/0008-6215(84)85069-7

Reference yield:

benzaldehyde (100-52-7) → benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methyl-α-D-glucopyranoside (116696-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc chloride

2: barium oxide

With zinc(II) chloride; barium(II) oxide;

Reference yield:

benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside (13343-63-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) + methyl iodide (74-88-4) → benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-methyl-α-D-glucopyranoside (116696-66-3)

Guidance literature:

With barium(II) oxide;

upstream raw materials:

benzyl 4,6-O-benzylidene-2-acetylamino-2-deoxy-α-D-glucopyranoside

N,N-dimethyl-formamide

methyl iodide

benzaldehyde

Downstream raw materials:

Benzoic acid (2R,3S,4R,5R,6S)-5-acetylamino-6-benzyloxy-4-methoxy-3-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-ylmethyl ester

benzyl 2-acetamido-6-O-benzoyl-2-deoxy-3-O-methyl-α-D-glucopyranoside

benzyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-methyl-α-D-glucopyranoside

benzyl 2-acetamido-2-deoxy-3-O-methyl-α-D-glucopyranoside

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