5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione

Base Information

• Chemical Name: 5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione
• CAS No.: 1522974-99-7
• Molecular Formula: C₂₃H₁₉NO₅
• Molecular Weight: 389.408

Synonyms:5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione

Chemical Property of 5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione

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Technology Process of 5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione

There total 1 articles about 5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

endo-1,4-Ethano-5-hydroxy-1,4,4a,9a-tetrahydro-9,10-anthraquinone (145212-76-6,131924-05-5) + 1-bromomethyl-4-nitro-benzene (100-11-8) → 5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione (1522974-99-7)

Guidance literature:

With silver(l) oxide; In dichloromethane; at 20 ℃; for 24h; Darkness; Inert atmosphere;

DOI:10.1021/ol403300a

Reference yield: 57.0%

5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione (1522974-99-7) → 5-(4-nitrobenzyloxy)-1,4-dihydro-1,4-ethanoanthracene-9,10-dione (1522975-05-8)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol403300a

Reference yield:

5-(4-nitrobenzyloxy)-1,4,4a,9a-tetrahydro-1,4-ethanoanthracene-9,10-dione (1522974-99-7) → C23H21NO4 (1522975-22-9) + C23H21NO3 (1522975-24-1) + endo-1,4-Ethano-5-hydroxy-1,4,4a,9a-tetrahydro-9,10-anthraquinone (145212-76-6,131924-05-5)

Guidance literature:

With ammonium formate; zinc; In methanol; aq. phosphate buffer; at 37 ℃; for 1h; pH=7.4;

DOI:10.1021/ol403300a

upstream raw materials:

endo-1,4-Ethano-5-hydroxy-1,4,4a,9a-tetrahydro-9,10-anthraquinone

1-bromomethyl-4-nitro-benzene

Downstream raw materials:

C₂₃H₂₁NO₄

C₂₃H₂₁NO₃

endo-1,4-Ethano-5-hydroxy-1,4,4a,9a-tetrahydro-9,10-anthraquinone

5-(4-nitrobenzyloxy)-1,4-dihydro-1,4-ethanoanthracene-9,10-dione

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