O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

Base Information

Chemical Name:O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate
CAS No.:1337538-34-7
Molecular Formula:C₂₃H₃₆O₄S₂
Molecular Weight:440.668
Hs Code.:

Synonyms:O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

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Chemical Property of O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

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Technology Process of O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

There total 3 articles about O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1337538-33-6
(S)-2-(benzyloxy)-1-((4R,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethanol

: 74-88-4
methyl iodide

: 1337538-34-7
O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

Guidance literature:: (S)-2-(benzyloxy)-1-((4R,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethanol; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

carbon disulfide; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

methyl iodide; In tetrahydrofuran; at 0 ℃; for 3h;
DOI:10.1016/j.tetasy.2011.07.007

Reference yield:

: 1337538-32-5
C₁₄H₂₈O₄

: 1337538-34-7
O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 18 h / Reflux

1.2: 2 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 1 h / 0 - 20 °C

2.3: 3 h / 0 °C

With sodium hydride; di(n-butyl)tin oxide; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetasy.2011.07.007

Reference yield:

: 100-39-0
benzyl bromide

: 1337538-34-7
O-((S)-2-(benzyloxy)-1-((4S,5R)-5-heptyl-2,2-dimethyl-1,3-dioxolan-4-yl)ethyl) S-methyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / toluene / 18 h / Reflux

1.2: 2 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 1 h / 0 - 20 °C

2.3: 3 h / 0 °C

With sodium hydride; di(n-butyl)tin oxide; In tetrahydrofuran; toluene;
DOI:10.1016/j.tetasy.2011.07.007