benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

Base Information

Chemical Name:benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside
CAS No.:912941-34-5
Molecular Formula:C₅₇H₈₅NO₁₁
Molecular Weight:960.302
Hs Code.:

Synonyms:benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

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Chemical Property of benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

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Technology Process of benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

There total 12 articles about benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 912941-33-4
benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-34-5
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 0.666667h;
DOI:10.1016/j.bmc.2006.05.051

Reference yield: 90.0%

: benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

: 912941-34-5
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 0.666667h;
DOI:10.3987/com-06-s(o)51

Reference yield:

: 912941-32-3
formylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-34-5
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 20 °C

2: 885.6 mg / CH₂Cl₂; diethyl ether / 20 °C

3: 90 percent / trifluoroacetic acid / CH₂Cl₂; H₂O / 0.67 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; trifluoroacetic acid; In diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.05.051