(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

Base Information

Chemical Name:(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate
CAS No.:517877-04-2
Molecular Formula:C₂₃H₃₅NO₆
Molecular Weight:421.534
Hs Code.:

Synonyms:(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

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Chemical Property of (1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

Chemical Property:

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Technology Process of (1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

There total 3 articles about (1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-73-9,85404-21-3
N-butylamine

: 404353-42-0
(1R,2R,3S,4R)-ethyl [3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco]heptfuran-5-enuronate

: 517877-04-2
(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

: 623559-41-1
ethyl 1,2-O-isopropylidene-3-O-benzyl-5-(N-butylamino)-5,6-dideoxy-β-L-ido-heptofuranuronate

Guidance literature:: In ethanol; at 25 ℃; Title compound not separated from byproducts;
DOI:10.1016/S0223-5234(02)01398-3

Reference yield:

: 108788-49-4
ethyl (E)-[3-O-benzyl-5,6-dideoxy-1,2-O-isopropylidene-α-D-gluco]-heptofuran-5-en-uronate

: 109-73-9,85404-21-3
N-butylamine

: 517877-04-2
(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

: 623559-41-1
ethyl 1,2-O-isopropylidene-3-O-benzyl-5-(N-butylamino)-5,6-dideoxy-β-L-ido-heptofuranuronate

Guidance literature:: at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2006.04.027

Reference yield:

: 23558-05-6
3-O-benzyl-1,2-O-isopropylidene-1,5-D-xylo-dialdofuranose

: 517877-04-2
(1R,2R,3S,4R,5R)-ethyl [3-O-benzyl-5-butylamino-5,6-dideoxy-1,2-Oisopropylidene]-α-D-gluco-heptofuranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / toluene / Heating

2: ethanol

In ethanol; toluene; 1: Wittig olefination / 2: Michael addition;
DOI:10.1081/CAR-120016857