C₅₄H₆₁NO₁₁

Base Information

Chemical Name:C₅₄H₆₁NO₁₁
CAS No.:350583-41-4
Molecular Formula:C₅₄H₆₁NO₁₁
Molecular Weight:900.078
Hs Code.:

C<sub>54</sub>H<sub>61</sub>NO<sub>11</sub>

Synonyms:C₅₄H₆₁NO₁₁

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Chemical Property of C₅₄H₆₁NO₁₁

Chemical Property:

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Technology Process of C₅₄H₆₁NO₁₁

There total 12 articles about C₅₄H₆₁NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 202390-86-1,949023-16-9
(2S,4S,5R)-3-Benzoyl-2-(p-methoxyphenyl)-4-phenyl-1,3-oxazolidine-5-carboxylic acid

: 350583-40-3
C₃₀H₄₂O₇

: 350583-41-4
C₅₄H₆₁NO₁₁

Guidance literature:: With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In dichloromethane; toluene; at 20 ℃; for 0.75h;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: C₃₉H₄₄O₇

: 350583-41-4
C₅₄H₆₁NO₁₁

Guidance literature:: Multi-step reaction with 12 steps

1: 76 percent / aq. NaOH / tetrahydrofuran / 48 h / Heating

2: 93 percent / pyridine / 96 h / 20 °C

3: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

4: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

5: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

6: 99 percent / sodium periodate / tetrahydrofuran; H₂O / 72 h / 20 °C

7: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C

8: 88 percent / NaBH₄ / methanol / 0.33 h / 0 °C

9: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C

10: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C

11: 91 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

12: 71 percent / 4-pyrrolidinopyridine; dicyclohexyl carbodiimide / toluene; CH₂Cl₂ / 0.75 h / 20 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium hydroxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-pyrrolidin-1-ylpyridine; 4-methylmorpholine N-oxide; triethylamine; dicyclohexyl-carbodiimide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; pyridine; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O

Reference yield:

: 350583-27-6
1,2-benzylidene-9,10-isopropylidene-5α-acetyltaxicin-I

: 350583-41-4
C₅₄H₆₁NO₁₁

Guidance literature:: Multi-step reaction with 10 steps

1: PBu₃; NEt₃; HCOOH / Pd(dba)2 / tetrahydrofuran / Heating

2: 67 percent / OsO₄; NMMO / tetrahydrofuran; H₂O; 2-methyl-propan-2-ol / 144 h / 20 °C

3: 61 percent / DIBALH / CH₂Cl₂; toluene / 0.5 h

4: 99 percent / sodium periodate / tetrahydrofuran; H₂O / 72 h / 20 °C

5: 92 percent / imidazole / dimethylformamide / 5 h / 20 °C

6: 88 percent / NaBH₄ / methanol / 0.33 h / 0 °C

7: 57 percent / n-butyllithium / tetrahydrofuran; hexane / 20 h / 20 °C

8: 48 percent / tert-butyl hydroperoxide; palladium(II) acetate / toluene / 72 h / 50 °C

9: 91 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

10: 71 percent / 4-pyrrolidinopyridine; dicyclohexyl carbodiimide / toluene; CH₂Cl₂ / 0.75 h / 20 °C

With 1H-imidazole; tert.-butylhydroperoxide; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; n-butyllithium; formic acid; tributylphosphine; tetrabutyl ammonium fluoride; palladium diacetate; diisobutylaluminium hydride; 4-pyrrolidin-1-ylpyridine; 4-methylmorpholine N-oxide; triethylamine; dicyclohexyl-carbodiimide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1002/1099-0690(200105)2001:9<1761::AID-EJOC1761>3.0.CO;2-O