(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Base Information

Chemical Name:(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide
CAS No.:1416475-87-0
Molecular Formula:C₁₉H₁₉NO₅
Molecular Weight:341.364
Hs Code.:

Synonyms:(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Suppliers and Price of (E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

There total 3 articles about (E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1-phenylbenzylhydroxylamine dioxalate salt

: 762-42-5
dimethyl acetylenedicarboxylate

: 1416475-87-0
(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Guidance literature:: With sodium acetate; In methanol; at 0 - 20 ℃;
DOI:10.1002/ejoc.201301739

Reference yield:

: 146495-24-1
N-(diphenylmethylene)aminoacetonitrile

: 1416475-87-0
(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 0.33 h / Inert atmosphere

2.1: sodium acetate trihydrate / methanol / 20 h / 0 - 20 °C / Inert atmosphere

With sodium acetate trihydrate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2012.11.010

Reference yield:

: 91-00-9
Benzhydrylamine

: 1416475-87-0
(E)-N-(1,4-dimethoxy-1,4-dioxobutan-2-ylidene)-1,1-diphenylmethanamine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / acetonitrile / 72 h / 20 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0.33 h / Inert atmosphere

3.1: sodium acetate trihydrate / methanol / 20 h / 0 - 20 °C / Inert atmosphere

With sodium acetate trihydrate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetasy.2012.11.010