C₂₄H₂₉NO₆

Base Information

• Chemical Name: C₂₄H₂₉NO₆
• CAS No.: 1333067-47-2
• Molecular Formula: C₂₄H₂₉NO₆
• Molecular Weight: 427.497
• Mol file: 1333067-47-2.mol

Synonyms:C₂₄H₂₉NO₆

Chemical Property of C₂₄H₂₉NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₂₉NO₆

There total 2 articles about C₂₄H₂₉NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C17H23NO6 (1333067-46-1) + benzyl bromide (100-39-0) → C24H29NO6 (1333067-47-2)

Guidance literature:

With silver(l) oxide; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere; Molecular sieve; Darkness;

DOI:10.1021/ja207496p

Reference yield:

(S)-4-benzyl-3-propionyl-2-oxazolidinone (131685-53-5,101711-78-8) → C24H29NO6 (1333067-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

1.2: -78 - 0 °C / Inert atmosphere

2.1: silver(l) oxide / dichloromethane / 48 h / 20 °C / Inert atmosphere; Molecular sieve; Darkness

With di-n-butylboryl trifluoromethanesulfonate; triethylamine; silver(l) oxide; In dichloromethane;

DOI:10.1021/ja207496p

Reference yield: 97.0%

C24H29NO6 (1333067-47-2) → C14H22O4 (1333067-48-3)

Guidance literature:

With methanol; lithium borohydride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 2h;

upstream raw materials:

C₁₇H₂₃NO₆

benzyl bromide

(S)-4-benzyl-3-propionyl-2-oxazolidinone

Downstream raw materials:

C₃₇H₅₀O₆Si