(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

Base Information

Chemical Name:(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane
CAS No.:947264-58-6
Molecular Formula:C₂₇H₃₈OSi₃
Molecular Weight:462.855
Hs Code.:

Synonyms:(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

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Technology Process of (3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

There total 2 articles about (3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13963-41-2
1,5-Bis(trimethylsilyl)-3-penta-1,4-diyn-3-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 947264-58-6
(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo0709753

Reference yield: 43.0%

: 947264-61-1
C₅H₃OSiC₁₆H₁₉

: 75-77-4
chloro-trimethyl-silane

: 947264-58-6
(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)bistrimethylsilane

: 215878-39-0
(3-(tert-butyldiphenylsilanyloxy)penta-1,4-diyne-1,5-diyl)trimethylsilane

Guidance literature:: C₅H₃OSiC₁₆H₁₉; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.5h; Further stages.;
DOI:10.1021/jo0709753