(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

Base Information

• Chemical Name: (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine
• CAS No.: 139016-43-6
• Molecular Formula: C₃₇H₄₂N₆
• Molecular Weight: 570.781

Synonyms:(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

Chemical Property of (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

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Technology Process of (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

There total 2 articles about (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2-vinylpyridine (100-69-6,25014-15-7,27476-03-5,329041-71-6) + 2,6-bis(aminomethyl)toluene (139016-44-7) → (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine (139016-43-6)

Guidance literature:

With acetic acid; In methanol; for 144h; Heating;

DOI:10.1021/ja00033a024

Reference yield:

2,6-dicyanotoluene (2317-22-8) → (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine (139016-43-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / LiAlH₄ / tetrahydrofuran; diethyl ether

2: 32 percent / AcOH / methanol / 144 h / Heating

With lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; methanol; diethyl ether;

DOI:10.1021/ja00033a024

Reference yield: 58.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-2-methyl-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine (139016-43-6) → {Cu2(C6(CH2N(C2H4C5H4N)2)2(CH3)H3)}(2+)*2PF6(1-)={Cu2(C6(CH2N(C2H4C5H4N)2)2(CH3)H3)}(PF6)2 (139016-46-9)

Guidance literature:

In dichloromethane; under Ar; stirring of diamine and copper complex in soln. for 40 min; addn. of Et2O, filtn., ppt. washed with Et2O, drying in vac., elem. anal.;

DOI:10.1021/ja00033a024

upstream raw materials:

2-vinylpyridine

2,6-bis(aminomethyl)toluene

2,6-dicyanotoluene

Downstream raw materials:

{Cu₂(C₆(CH₂N(C₂H₄C₅H₄N)2)2(CH₃)H₃)}⁽²⁺⁾*2PF₆^(1-)={Cu₂(C₆(CH₂N(C₂H₄C₅H₄N)2)2(CH₃)H₃)}(PF₆)2

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