2,6-DICYANOTOLUENE

Base Information

Chemical Name:2,6-DICYANOTOLUENE
CAS No.:2317-22-8
Molecular Formula:C9H6 N2
Molecular Weight:142.16
Hs Code.:2926909090
Mol file:2317-22-8.mol

Synonyms:Isophthalonitrile,2-methyl- (6CI,7CI,8CI); 1,3-Dicyano-2-methylbenzene; 2,6-Dicyanotoluene;2-Methylisophthalonitrile

Suppliers and Price of 2,6-DICYANOTOLUENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methylisophthalonitrile
100mg
$ 75.00

Sigma-Aldrich
2,6-Dicyanotoluene 97%
25g
$ 605.00

Sigma-Aldrich
2,6-Dicyanotoluene 97%
5g
$ 370.00

Matrix Scientific
2-Methylisophthalonitrile >95%
1g
$ 228.00

Matrix Scientific
2-Methylisophthalonitrile >95%
5g
$ 420.00

Crysdot
2-Methylisophthalonitrile 95+%
5g
$ 519.00

American Custom Chemicals Corporation
3-PHTHALODINITRILE 95.00%
1G
$ 722.80

American Custom Chemicals Corporation
3-PHTHALODINITRILE 95.00%
10G
$ 1585.35

American Custom Chemicals Corporation
3-PHTHALODINITRILE 95.00%
5G
$ 1115.96

Alichem
2-Methylisophthalonitrile
25g
$ 2110.50

Total 17 raw suppliers

Chemical Property of 2,6-DICYANOTOLUENE

Chemical Property:

Vapor Pressure:0.00113mmHg at 25°C
Melting Point:135-137 °C(lit.)
Refractive Index:1.6211 (estimate)
Boiling Point:125-130 °C2 mm Hg(lit.)
Flash Point:117.2°C
PSA：47.58000
Density:1.12g/cm³
LogP:1.73836

Purity/Quality:

97% ^*data from raw suppliers

2-Methylisophthalonitrile ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 20/21/22-36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Uses 2,6-Dicyanotoluene was used in the synthesis of E-2-(2,6-dcyanophenyl)-N,N-dimethylethenamine by undergoing condensation with dimethylformamide dimethyl acetal (DMFDMA).

Technology Process of 2,6-DICYANOTOLUENE

There total 6 articles about 2,6-DICYANOTOLUENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 118-69-4
2,6-dichlorotoluene

: 544-92-3
copper(I) cyanide

: 2317-22-8
2,6-dicyanotoluene

Guidance literature:: With 1-methyl-pyrrolidin-2-one; for 18h; Heating;
DOI:10.1055/s-1990-26963

Reference yield:

: 54454-12-5
(3-chloro-2-methylphenyl)carbonitrile

: 544-92-3
copper(I) cyanide

: 2317-22-8
2,6-dicyanotoluene

Guidance literature:: With pyridine; at 230 - 240 ℃;
DOI:10.1021/ja01465a044

Reference yield:

: 626-17-5
benzene-1,3-dicarbonitrile

: 74-88-4
methyl iodide

: 2317-22-8
2,6-dicyanotoluene

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -96 deg C, 0.5 h, 2.) 10 equiv of CH₃I, -96 deg C to room temp.;
DOI:10.1021/jo00134a038