C₃₅H₄₈O₇Si

Base Information

Chemical Name:C₃₅H₄₈O₇Si
CAS No.:1261148-45-1
Molecular Formula:C₃₅H₄₈O₇Si
Molecular Weight:608.847
Hs Code.:

C<sub>35</sub>H<sub>48</sub>O<sub>7</sub>Si

Synonyms:C₃₅H₄₈O₇Si

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Chemical Property of C₃₅H₄₈O₇Si

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Technology Process of C₃₅H₄₈O₇Si

There total 18 articles about C₃₅H₄₈O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1261148-58-6
C₃₀H₄₂O₅Si

: 623-47-2
propynoic acid ethyl ester

: 1261148-45-1
C₃₅H₄₈O₇Si

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 25 ℃; for 23h; Inert atmosphere;
DOI:10.1021/ja109531d

Reference yield:

: 1227265-23-7
C₃₁H₃₆O₄Si

: 1261148-45-1
C₃₅H₄₈O₇Si

Guidance literature:: Multi-step reaction with 18 steps

1.1: diethyl ether / 1 h / -78 °C / Inert atmosphere

2.1: 20 % Pd(OH)2/C; hydrogen / ethanol; ethyl acetate / 18 h / 25 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 18 h / 25 °C / Inert atmosphere

4.1: dichloromethane / 4 h / 25 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane / -78 - 0 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.33 h / -20 °C / Molecular sieve; Inert atmosphere

7.2: 1 h / -20 °C / Inert atmosphere

8.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 9 h / 0 - 25 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

9.2: 1 h / -78 - 0 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

11.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

12.1: 1H-imidazole / dichloromethane / 0 - 25 °C / Inert atmosphere

13.1: borane-THF / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13.2: 1 h / 0 °C

14.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

15.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

16.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 12 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

17.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

18.1: 4-methyl-morpholine / dichloromethane / 23 h / 25 °C / Inert atmosphere

With 4-methyl-morpholine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tetrapropylammonium perruthennate; borane-THF; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2S,3S)-tartrate; [bis(acetoxy)iodo]benzene; 20 % Pd(OH)2/C; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; 1.1: Grignard reaction / 7.1: Sharpless epoxidation / 7.2: Sharpless epoxidation / 9.1: Whiting reaction / 9.2: Whiting reaction;
DOI:10.1021/ja109531d

Reference yield:

: C₃₃H₅₀O₅Si₂

: 1261148-45-1
C₃₅H₄₈O₇Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 - 0 °C / Inert atmosphere

2.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.33 h / -20 °C / Molecular sieve; Inert atmosphere

2.2: 1 h / -20 °C / Inert atmosphere

3.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 9 h / 0 - 25 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 0.5 h / 0 °C / Inert atmosphere

4.2: 1 h / -78 - 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

6.1: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

7.1: 1H-imidazole / dichloromethane / 0 - 25 °C / Inert atmosphere

8.1: borane-THF / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

8.2: 1 h / 0 °C

9.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

10.1: tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

11.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 12 h / 0 - 25 °C / Molecular sieve; Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

13.1: 4-methyl-morpholine / dichloromethane / 23 h / 25 °C / Inert atmosphere

With 4-methyl-morpholine; 1H-imidazole; titanium(IV) isopropylate; tetrapropylammonium perruthennate; borane-THF; diethyl (2S,3S)-tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; 2.1: Sharpless epoxidation / 2.2: Sharpless epoxidation / 4.1: Whiting reaction / 4.2: Whiting reaction;
DOI:10.1021/ja109531d