4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

Base Information

Chemical Name:4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate
CAS No.:952410-53-6
Molecular Formula:C₂₅H₂₉N₄O₆P
Molecular Weight:512.502
Hs Code.:

Synonyms:4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

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Chemical Property of 4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

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Technology Process of 4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

There total 4 articles about 4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.1%

: 952410-50-3
5-(6-chloro-2,4-dimethoxypyrimidin-5-yl)-5-oxopentanyl dibenzyl phosphate

: 952410-53-6
4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

Guidance literature:: With hydrazine; In methanol; for 18h; Heating;
DOI:10.1021/jo070982r

Reference yield:

: 50651-75-7
silver dibenzylphosphate

: 952410-53-6
4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 percent / toluene / 24 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.2: 25.6 percent / tetrahydrofuran / -78 - -40 °C

3.1: 58.1 percent / hydrazine / methanol / 18 h / Heating

With n-butyllithium; hydrazine; In tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1021/jo070982r

Reference yield:

: 14660-52-7
ethyl 5-bromovalerate

: 952410-53-6
4-(4,6-dimethoxy-1H-pyrazolo[3,4-d]pyrimidin-3-yl)butyl dibenzyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 percent / toluene / 24 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.2: 25.6 percent / tetrahydrofuran / -78 - -40 °C

3.1: 58.1 percent / hydrazine / methanol / 18 h / Heating

With n-butyllithium; hydrazine; In tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1021/jo070982r