12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

Base Information

Chemical Name:12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene
CAS No.:793670-84-5
Molecular Formula:C₂₄H₂₃NO
Molecular Weight:341.453
Hs Code.:

Synonyms:12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

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Technology Process of 12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

There total 1 articles about 12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 81059-37-2
cis-9,10-dihydro-9,10-anthracenedicarboxaldehyde

: 2393-23-9
4-methoxy-benzylamine

: 793670-84-5
12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

Guidance literature:: With sodium cyanoborohydride; acetic acid; In dichloromethane; at -78 - 20 ℃;
DOI:10.1081/SCC-200030972

Reference yield: 93.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 793670-84-5
12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

: 793670-85-6
12-benzyloxycarbonyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

Guidance literature:: In benzene; for 6h; Heating;
DOI:10.1081/SCC-200030972

Reference yield:

: 793670-84-5
12-(p-methoxyphenyl)methyl-9,10-dihydro-9,10-(methaniminomethano)anthracene

: 24686-27-9
9,10-dihydro-9,10-(methaniminomethano)anthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / benzene / 6 h / Heating

2: 67 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 1.5 h / 20 °C

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; benzene;
DOI:10.1081/SCC-200030972