1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE

Base Information

Chemical Name:1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE
CAS No.:102821-91-0
Molecular Formula:C₁₈H₂₁N₃O
Molecular Weight:295.384
Hs Code.:
Mol file:102821-91-0.mol

Synonyms:3-amino-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenzazepine

Suppliers and Price of 1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-(3-Amino-10,11-dihydro-dibenzo[b,f]azepin-5-yl)-2-dimethylamino-ethanone
1g
$ 378.00

Matrix Scientific
1-(3-Amino-10,11-dihydro-dibenzo[b,f]azepin-5-yl)-2-dimethylamino-ethanone
500mg
$ 225.00

Crysdot
1-(3-Amino-10,11-dihydro-5H-dibenzo[b,f]azepin-5-yl)-2-(dimethylamino)ethanone 97%
5g
$ 874.00

American Custom Chemicals Corporation
1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE 95.00%
500MG
$ 762.30

Total 4 raw suppliers

Chemical Property of 1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE

Chemical Property:

Melting Point:124-126 °C
Boiling Point:535.1±50.0 °C(Predicted)
PKA:6.99±0.28(Predicted)
Density:1.187±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

1-(3-Amino-10,11-dihydro-dibenzo[b,f]azepin-5-yl)-2-dimethylamino-ethanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi,Xn
Statements: 22

MSDS Files:

Useful:

Uses 1-(3-Amino-10,11-dihydro-dibenzo[b,f]azepin-5-yl)-2-dimethylamino-ethanone (CAS# 102821-91-0) can be used for its immunochemical properties toward anti-arrhythmic activity.

Technology Process of 1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE

There total 5 articles about 1-(3-AMINO-10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-2-DIMETHYLAMINO-ETHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 78816-67-8
[5-(2-Dimethylamino-acetyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl]-carbamic acid ethyl ester; hydrochloride

: 102821-91-0
3-amino-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenzazepine

Guidance literature:: With sodium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1007/BF00766590

Reference yield:

: 10464-35-4
3-amino-10,11-dihydro-5H-dibenzazepine

: 102821-91-0
3-amino-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂CO₃ / acetone; H₂O / 1.5 h

2: toluene / 4 h / Heating

3: toluene / 4 h / 70 - 110.8 °C

4: HCl in isopropanol / propan-2-ol

5: 75 percent / 4 M NaOH / ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; sodium carbonate; In ethanol; water; isopropyl alcohol; acetone; toluene;

Reference yield:

: 78816-40-7
3-carbethoxyamino-10,11-dihydro-5H-dibenzazepine

: 102821-91-0
3-amino-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenzazepine

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 4 h / Heating

2: toluene / 4 h / 70 - 110.8 °C

3: HCl in isopropanol / propan-2-ol

4: 75 percent / 4 M NaOH / ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; In ethanol; isopropyl alcohol; toluene;