3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

Base Information

Chemical Name:3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine
CAS No.:220194-94-5
Molecular Formula:C₂₅H₂₆N₄O₂
Molecular Weight:414.507
Hs Code.:

Synonyms:3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

Suppliers and Price of 3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

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Technology Process of 3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

There total 3 articles about 3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 220194-92-3
5-dimethylaminoacetyl-3-(4-nitrobenzoylamino)-10,11-dihydro-5H-dibenz[b,f]azepine

: 220194-94-5
3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

Guidance literature:: With hydrazine hydrate; nickel; In ethanol; acetone; for 2h; Heating;
DOI:10.1007/BF02539228

Reference yield:

: 102821-91-0
3-amino-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenzazepine

: 220194-94-5
3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / sodium carbonate / ethanol; acetone / 1 h / 10 - 12 °C

2: 73 percent / hydrazine hydrate / Raney nickel / ethanol; acetone / 2 h / Heating

With sodium carbonate; hydrazine hydrate; nickel; In ethanol; acetone; 1: Acylation / 2: Reduction;
DOI:10.1007/BF02539228

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 220194-94-5
3-(4-aminobenzoylamino)-5-dimethylaminoacetyl-10,11-dihydro-5H-dibenz[b,f]azepine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / sodium carbonate / ethanol; acetone / 1 h / 10 - 12 °C

2: 73 percent / hydrazine hydrate / Raney nickel / ethanol; acetone / 2 h / Heating

With sodium carbonate; hydrazine hydrate; nickel; In ethanol; acetone; 1: Acylation / 2: Reduction;
DOI:10.1007/BF02539228