5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

Base Information

Chemical Name:5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde
CAS No.:1189353-30-7
Molecular Formula:C₂₀H₂₆N₂O₄S
Molecular Weight:390.503
Hs Code.:

Synonyms:5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

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Chemical Property of 5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

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Technology Process of 5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

There total 2 articles about 5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189353-29-4
(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)methanol

: 1189353-30-7
5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; Cooling with ice;

Reference yield:

: 1189351-76-5
methyl 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoate

: 1189353-30-7
5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 0 °C / Cooling with ice

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Cooling with ice

3: Dess-Martin periodane / dichloromethane / 0 °C / Cooling with ice

With lithium aluminium tetrahydride; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane;

Reference yield: 90.0%

: 503-29-7
azetidine

: 1189353-30-7
5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

: 1189353-33-0
3-(azetidin-1-ylmethyl)-4-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}-N,N-dimethylaniline

Guidance literature:: azetidine; 5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 20 ℃; Cooling with ice;

With water; sodium hydrogencarbonate; In dichloromethane;