1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

Base Information

Chemical Name:1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol
CAS No.:1189353-31-8
Molecular Formula:C₂₁H₃₀N₂O₄S
Molecular Weight:406.546
Hs Code.:

Synonyms:1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

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Chemical Property of 1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

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Technology Process of 1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

There total 3 articles about 1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1189353-30-7
5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde

: 75-16-1
methylmagnesium bromide

: 1189353-31-8
1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

Guidance literature:: 5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}benzaldehyde; methylmagnesium bromide; In tetrahydrofuran; toluene; at 0 ℃; Cooling with ice;

With citric acid; In tetrahydrofuran; toluene;

Reference yield:

: 1189351-76-5
methyl 5-(dimethylamino)-2-(7-hydroxy-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzoate

: 1189353-31-8
1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran / 0 °C / Cooling with ice

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Cooling with ice

3: Dess-Martin periodane / dichloromethane / 0 °C / Cooling with ice

4: tetrahydrofuran; toluene / 0 °C / Cooling with ice

With lithium aluminium tetrahydride; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1189353-29-4
(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)methanol

: 1189353-31-8
1-(5-(dimethylamino)-2-{7-[(2-methoxyethoxy)methoxy]-4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl}phenyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 0 °C / Cooling with ice

2: tetrahydrofuran; toluene / 0 °C / Cooling with ice

With Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene;