(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

Base Information

Chemical Name:(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione
CAS No.:812679-22-4
Molecular Formula:C₁₄H₁₈N₂O₂
Molecular Weight:248.293
Hs Code.:

Synonyms:(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

Suppliers and Price of (3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

Chemical Property:

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Technology Process of (3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

There total 1 articles about (3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (3S,6R,1'R/S)-N,N'-bis-(4-methoxybenzyl)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-2,5-dione

: 812679-22-4
(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

Guidance literature:: With ammonium cerium(IV) nitrate; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1039/b500566c

Reference yield:

: 812679-22-4
(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

: (2R,3S)-2-amino-2,3-dideuterio-3-phenylpropionic acid

: (2S,3R)-2-amino-2,3-dideuterio-3-phenylpropionic acid hydrochloride

: 17498-50-9,25616-14-2,31320-20-4
L-valine hydrochloride

Guidance literature:: With hydrogenchloride; for 36h; Title compound not separated from byproducts; Heating;
DOI:10.1039/b500566c

Reference yield:

: 812679-22-4
(3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione

: 67-56-1
methanol

: (2R,3S)-2-amino-2,3-dideuterio-3-phenylpropionic acid methyl ester

: (2S,3R)-2-amino-2,3-dideuterio-3-phenylpropionic acid methyl ester

: 6306-52-1
L-valine methylester hydrochloride

Guidance literature:: (3S,6R,1'R)-3-deuterio-3-(deuteriophenylmethyl)-6-isopropyl-piperazine-2,5-dione; With hydrogenchloride; for 36h; Heating;

methanol; With thionyl chloride; at 20 ℃; for 12h; Title compound not separated from byproducts;
DOI:10.1039/b500566c