tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate

Base Information

• Chemical Name: tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate
• CAS No.: 303069-17-2
• Molecular Formula: C₁₅H₂₆N₂O₆P₂
• Molecular Weight: 392.329
• Mol file: 303069-17-2.mol

Synonyms:tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate

Chemical Property of tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate

Chemical Property:

Purity/Quality:

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Technology Process of tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate

There total 1 articles about tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

pyridine-2-carbaldehyde (1121-60-4) + tetraethyl (aminomethylene)bis(phosphonate) (80474-99-3) → tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate (303069-17-2)

Guidance literature:

In benzene; for 4h; Heating;

DOI:10.1016/S0040-4020(00)00570-6

Reference yield: 60.0%

4-methyl-benzaldehyde (104-87-0) + tetraethyl (E)-N-(2-pyridinemethyliden)aminomethyldiphosphonate (303069-17-2) → (1E,3E)-3-(diethoxyphosphoryl)-4-(4-methylphenyl)-1-(2-pyridyl)-2-azabuta-1,3-diene

Guidance literature:

With caesium carbonate; In tetrahydrofuran; isopropyl alcohol; at 20 ℃;

DOI:10.1016/S0040-4020(00)00570-6

upstream raw materials:

pyridine-2-carbaldehyde

tetraethyl (aminomethylene)bis(phosphonate)