[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

Base Information

Chemical Name:[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane
CAS No.:195436-19-2
Molecular Formula:C₃₀H₄₀O₇Si
Molecular Weight:540.729
Hs Code.:

Synonyms:[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

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Chemical Property of [(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

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Technology Process of [(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

There total 12 articles about [(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2878-55-9
3,4-(methylenedioxy)benzyl α-ethoxyethyl ether

: 195436-19-2
[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 5 steps

2: 80 percent / KH / dimethylformamide / 2 h / Ambient temperature

3: 92 percent / 0.5 N HCl / tetrahydrofuran / 7.25 h / Ambient temperature

4: 50.7 mg / KH / tetrahydrofuran / 1 h / -78 °C

5: 22.4 mg / CSA / CH₂Cl₂ / 34 h / Ambient temperature

With hydrogenchloride; camphor-10-sulfonic acid; potassium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00373-6

Reference yield:

: 195436-27-2
4-Benzyloxy-5-(1-ethoxy-ethoxymethyl)-benzo[1,3]dioxole

: 195436-19-2
[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 0.5 N HCl / tetrahydrofuran / 7.25 h / Ambient temperature

2: 50.7 mg / KH / tetrahydrofuran / 1 h / -78 °C

3: 22.4 mg / CSA / CH₂Cl₂ / 34 h / Ambient temperature

With hydrogenchloride; camphor-10-sulfonic acid; potassium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4020(97)00373-6

Reference yield:

: 160094-76-8
4-hydroxy-5-(1-ethoxyethyl)oxymethyl-1,3-benzodioxolane

: 195436-19-2
[(3aS,4S,7R,7aS)-7-(4-Benzyloxy-benzo[1,3]dioxol-5-ylmethoxy)-2,2-dimethyl-3a,4,7,7a-tetrahydro-benzo[1,3]dioxol-4-yloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / KH / dimethylformamide / 2 h / Ambient temperature

2: 92 percent / 0.5 N HCl / tetrahydrofuran / 7.25 h / Ambient temperature

3: 50.7 mg / KH / tetrahydrofuran / 1 h / -78 °C

4: 22.4 mg / CSA / CH₂Cl₂ / 34 h / Ambient temperature

With hydrogenchloride; camphor-10-sulfonic acid; potassium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)00373-6