diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

Base Information

Chemical Name:diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate
CAS No.:1201947-36-5
Molecular Formula:C₁₆H₁₈ClN₃O₄
Molecular Weight:351.79
Hs Code.:

Synonyms:diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

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Chemical Property of diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

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Technology Process of diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

There total 2 articles about diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 35022-42-5
2-chlorobenzoyl cyanide

: 1201947-36-5
diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

Guidance literature:: With triphenylphosphine; In toluene; at 90 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b913196e

Reference yield: 80.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 609-65-4
o-chlorobenzoyl chloride

: potassium ferrocyanide

: 1201947-36-5
diisopropyl (Z)-2-((2-chlorophenyl)(cyano)methylene)hydrazine-1,1-dicarboxylate

Guidance literature:: o-chlorobenzoyl chloride; potassium ferrocyanide; at 160 ℃; for 3h;

di-isopropyl azodicarboxylate; With triphenylphosphine; In toluene; at 20 - 90 ℃; for 1h; stereoselective reaction;
DOI:10.1080/10426507.2012.658983