B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

Base Information

Chemical Name:B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)
CAS No.:74721-87-2
Molecular Formula:C₈H₁₅B₁₀Cl₅N₃P₃
Molecular Weight:531.523
Hs Code.:

B<sub>10</sub>H<sub>10</sub>C<sub>2</sub>C<sub>6</sub>H<sub>5</sub>(N<sub>3</sub>P<sub>3</sub>Cl<sub>5</sub>)

Synonyms:B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

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Technology Process of B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

There total 1 articles about B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 940-71-6,16422-79-0
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine

: 41655-52-1
1-lithia-2-phenyl-1,2-dicarba-closo-dodecaborane

: 74721-87-2
B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

Guidance literature:: In diethyl ether; room temp., 12 h; evapd., sublimed at 60-100°C, 0.05 torr, recrystd. with hexane/chloroform, elem. anal.;
DOI:10.1021/ja00392a019

Reference yield: 95.0%

: 110-89-4
piperidine

: 74721-87-2
B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

: 84393-77-1
P₃N₃(NC₅H₁₀)5(C₂(C₆H₅)B₉H₁₀)^(1-)*H₂NC₅H₁₀⁽¹⁺⁾ = [P₃N₃(NC₅H₁₀)5(C₂(C₆H₅)B₉H₁₀)][H₂NC₅H₁₀]

Guidance literature:: In benzene; soln. of the B-compd. treated with piperidine for 28 h at 80°C; cooled, filtered, solvent evapd., washed with EtOH, recrystd. from toluene, elem. anal., NMR, IR;
DOI:10.1021/ja00343a040

Reference yield: 80.0%

: 74721-87-2
B₁₀H₁₀C₂C₆H₅(N₃P₃Cl₅)

: 420-87-1
sodium 2,2,2-trifluoroethanolate

: 28212-50-2
[NP(CF₃CH₂O)2]2[NP(CF₃CH₂O)B₁₀H₁₀C₂C₆H₅]

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; 66°C, 120 h; evapd., neutralized with HCl, ppt. filtered, washed with water, dried, purified by fractional pptn., elem. anal.;
DOI:10.1021/ja00392a019