thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester

Base Information

• Chemical Name: thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester
• CAS No.: 1048377-95-2
• Molecular Formula: C₂₀H₃₁NO₆S
• Molecular Weight: 413.535

Synonyms:thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester

Chemical Property of thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester

Chemical Property:

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Technology Process of thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester

There total 1 articles about thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

[2-(3,5-dimethoxy-benzyloxy)-ethyl]-(2-hydroxy-ethyl)-carbamic acid tert-butyl ester (1048377-96-3) + tiolacetic acid (507-09-5) → thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester (1048377-95-2)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1021/ol8013667

Reference yield:

thiolacetic acid 2-{tert-butoxycarbonyl-[2-(3,5-dimethoxy-benzyloxy)-ethyl]-amino}-ethyl ester (1048377-95-2) → [2-(3,5-dimethoxy-benzyloxy)-ethyl]-(2-mercapto-ethyl)-amine (1048377-93-0)

Guidance literature:

With acetyl chloride; In methanol; at -78 ℃; Inert atmosphere;

DOI:10.1021/ol8013667

upstream raw materials:

[2-(3,5-dimethoxy-benzyloxy)-ethyl]-(2-hydroxy-ethyl)-carbamic acid tert-butyl ester

tiolacetic acid

Downstream raw materials:

[2-(3,5-dimethoxy-benzyloxy)-ethyl]-(2-mercapto-ethyl)-amine

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